期刊
MACROMOLECULAR RAPID COMMUNICATIONS
卷 25, 期 1, 页码 297-301出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/marc.200300187
关键词
combinatorial chemistry; electrochemistry; mesoporous; photochemistry; zinc oxide
Automated electrochemical synthesis was used to create combinatorial libraries of mesoporous materials using tri-block copolymers as structure directing agents (SDA). An example library of 56 ZnO samples was synthesized, varying concentrations (0-15 wt.-%) of poly(ethylene oxide)-block-poly(propylene oxide)-block-poly(ethylene oxide) - EO20 PO70EO20. High-throughput photoelectrochemical screening for the measurement of water-splitting photocatalysis identified peak performance at 3 wt.-% of the SDA. Lamellar structures and disordered mesopores were observed by TEM and XRD.
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