期刊
ORGANIC LETTERS
卷 6, 期 8, 页码 1265-1268出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol049805s
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资金
- NIGMS NIH HHS [GM 50101] Funding Source: Medline
[GRAPHICS] The radicals formed in Mn(III)-based oxidative free-radical cyclizations of beta-keto esters and malonate esters can be trapped with sodium azide and Mn(ill) to give cyclic and bicyclic azides in 30-80% yield. Reduction of the azide gives bi- and tricyclic lactams.
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