期刊
ORGANIC PROCESS RESEARCH & DEVELOPMENT
卷 8, 期 3, 页码 535-538出版社
AMER CHEMICAL SOC
DOI: 10.1021/op034181b
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A series of synthetic transformations were successfully and safely scaled up to multigram quantities using focused microwave irradiation with a continuous flow reaction cell that was developed in-house and which can be easily adapted to commercially available instrumentation. The representative reactions that were investigated included aromatic nucleophilic substitution (SNAr),. esterification, and the Suzuki cross-coupling reaction. In general, the product yields were equivalent to or greater than those run under conventional thermal heating conditions.
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