期刊
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
卷 -, 期 10, 页码 1992-1995出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejic.200300965
关键词
lanthanides; macrocyclic ligands; metallocenes; porphyrinoids; samarium
Modifying the porphyrinogen framework in lanthanide porphyrinogen complexes by trans-N,N'-dimethylation results in Sm-II and Sm-III derivatives that are remarkably simple in structure and formulation, and are amenable to highly controllable further reaction chemistry. The Sm-II bis(tetrahydrofuran) adduct, Sm-III chloride and bis(trimethylsilyl)amide complexes have been synthesised and characterised by elemental analysis, H-1 and C-13 NMR spectroscopy and X-ray crystal structure determinations. ((C) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004).
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