期刊
MACROMOLECULAR RAPID COMMUNICATIONS
卷 25, 期 12, 页码 1186-1190出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/marc.200400053
关键词
3D-TEM; electron tomography; in situ silica; nanocomposites; natural rubber
The three dimansional (3D) nanostructure of particulate in rubber (NR) were observed for the first time by use of 3D transmission electron tomography. The method enabled us to visualize and evaluate structural charachteristics in 3D space, such as the size and the volume of in situ silica generated in the NR matrix by the sol-gel reaction of tetraethoxysilane, at nanometer scale resolution.
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