期刊
APPLIED SURFACE SCIENCE
卷 263, 期 -, 页码 769-776出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.apsusc.2012.09.163
关键词
Ceria; Mixed-solvothermal; Superstructure; CO oxidization
类别
资金
- China Postdoctoral Science Foundation [20100470841]
- Natural Science Foundation of Jiangxi Province [2010BJB01100]
- National Basic Research Program of China [2011CB933700, 2010CB934700]
- Chinese Academy of Sciences
- National Natural Science Foundation of China [20971118]
Highly uniform pancake-like CeOHCO3 hierarchical microstructures have been successfully prepared by a simple gelatin-assisted mixed-solvothermal route. Ceria hierarchical microstructures with similar morphology were obtained after thermal treatment of the CeOHCO3 hierarchical microstructures at 700 degrees C for 4 h. The CeOHCO3 microstructures can be selectively obtained by varying the composition of solvent, concentration of gelatin and triethylenetetramine (TETA). The as-prepared products were characterized by X-ray powder diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electronic microscope (SEM), transmission electron microscopy (TEM), high-resolution TEM (HRTEM) and selected area electron diffraction (SAED). The possible formation process of the CeOHCO3 microstructures was briefly discussed. Gold coated ceria microstructures were also prepared which show excellent catalytic activity in the conversion of carbon monoxide, the T-50 and T-90 are at 240 degrees C and 300 degrees C, respectively. (C) 2012 Elsevier B.V. All rights reserved.
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