期刊
APPLIED SURFACE SCIENCE
卷 255, 期 12, 页码 6415-6420出版社
ELSEVIER
DOI: 10.1016/j.apsusc.2009.02.030
关键词
ZnO; Nanorod; Electrodeposition; Aqueous solution method; Seed layer
类别
资金
- Key Project of Chinese Ministry of Education [208008]
- Technology Development Foundation Plan Project of Tianjin Colleges [20071204]
- Science Technology Plan Project of Chinese Ministry of Construction [2007-K1-30]
ZnO nanorod arrays on ZnO-coated seed layers were fabricated by aqueous solution method using zinc nitrate and hexamethylenetetramine at low temperature. The seed layers were coated on ITO substrates by electrochemical deposition technique, and their textures were dominated by controlling the deposition parameters, such as deposition potential and electrolyte concentration. The effects of the electrodeposited seed layers and the growing parameters on the structures and properties of ZnO nanorod arrays were primarily discussed. The orientation and morphology of both the seed layer and successive nanorods were analyzed by using X-ray diffraction (XRD), SEM and TEM. The results show that the seed layer deposited at -700 mV has evenly distributed crystallites and (0 0 2) preferred orientation; the density of resultant nanorods is high and ZnO nanorods stand completely perpendicular onto substrates. Meanwhile, the size of nanorods quite also depends on the growth solution, and the higher concentration of growth solution primary leads to a large diameter of the ZnO nanorods. (C) 2009 Elsevier B.V. All rights reserved.
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