期刊
APPLIED SURFACE SCIENCE
卷 255, 期 23, 页码 9327-9332出版社
ELSEVIER
DOI: 10.1016/j.apsusc.2009.07.030
关键词
Surface imprinting; Core-shell; Microspheres; Trans-resveratrol
类别
资金
- Natural Science Foundation of Hunan Province, China [08JJ4004]
- Research Foundation of Education Bureau of Hunan Province, China [07B061]
A novel core-shell molecularly imprinting microspheres (MIMs) with trans-resveratrol as the template molecule; acrylamide ( AA) as functional monomer and ethylene glycol dimethacrylate ( EGDMA) as cross-linker, was prepared based on SiO2 microspheres with surface imprinting technique. These core shell trans-resveratrol imprinted microspheres were characterized by infrared spectra (IR), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and high performance liquid chromatography ( HPLC). The results showed that these core-shell imprinted microspheres, which take on perfect spherical shape with average shell thickness of 150 nm, exhibit especially selective recognition for trans-resveratrol. These imprinted microspheres were applied as solid-phase extraction materials for selective extraction of trans-resveratrol from giant knotweed extracting solution successfully. (C) 2009 Elsevier B.V. All rights reserved.
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