期刊
ORGANIC LETTERS
卷 6, 期 20, 页码 3649-3652出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol048328a
关键词
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资金
- NIGMS NIH HHS [R01 GM63167-01A1] Funding Source: Medline
A mild and general cross-coupling reaction of 2-indolylsilanols has been developed. The experimental variables that lead to successful coupling are (1) the use of sodium tert-butoxide as the activator, (2) the use of copper(l) iodide in stoichiometric quantities, and (3) the use of Pd-2(dba)(3).CHCl3 as the catalyst. Under these conditions N-(Boc)-2-indolyldimethylsilanol reacts with a variety of aromatic iodides to afford the coupling products in good yield (70-84%).
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