期刊
FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT
卷 21, 期 10, 页码 935-941出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/02652030400007252
关键词
Sudan I (1 phenylazo-2-naphthol); Soxtec; GPC; HPLC; UV/VIS; LC/MS; ESI; chilli; hot chilli products
A simple and rapid method is reported for the routine determination 1-phenylazo-2-naphthol (Sudan I) in chilli powder and in chilli-containing food products. The method involved Soxtec extraction from the products followed by high-pressure gel permeation chromatographic clean-up collecting the appropriate fraction. Analysis of this fraction was by HPLC with U VI VIS detection. The limit of detection was 7 mug kg(-1) and the limit of quantification was 13 mug kg(-1). The identity of Sudan I in food products was established by electrospray LC/MS with MS/MS confirmation. From a small survey of 30 retail samples, 11 samples of crushed chilli, Italian pasta, chilli-snack and vegetable sauce contained levels of Sudan I ranging from 24 to 5591 mug kg(-1).
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