期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 69, 期 20, 页码 6790-6795出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo0492057
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资金
- NCI NIH HHS [CA 82169-01] Funding Source: Medline
A selection of ortho-substituted aryl siloxanes have been prepared by directed orthometalation protocols. These siloxanes can be prepared in high yields and purity by use of a diverse selection of ortho-directing groups and electrophilic siloxane derivatives. The siloxanes are employed in palladium-catalyzed cross-coupling reactions with aryl bromides to generate unsymmetrical orthosubstituted biaryls in good to excellent yields.
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