期刊
ORGANIC LETTERS
卷 6, 期 21, 页码 3865-3868出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol048381z
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资金
- NCI NIH HHS [CA 103339] Funding Source: Medline
- NIGMS NIH HHS [GM 38907] Funding Source: Medline
An efficient synthesis of the C(11)-C(29) fragment 31 of amphidinolide F has been accomplished via a diastereoselective [3+2]-annulation reaction of allylsilane 5 and ethyl glyoxylate to prepare the key tetrahydrofuran 15 and a highly stereoselective methyl ketone aldol reaction to generate the C(11)-C(16) segment.
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