期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 346, 期 13-15, 页码 1793-1797出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.200404146
关键词
alkynes; arenesulfonyl chlorides; C-C cross coupling; homogeneous catalysis; palladium; tri(t-butyl)phosphine ligand
For the first time, conditions have been found for the palladium-catalyzed desulfitative carbon-carbon cross-coupling of arenesulfonyl chlorides with aryl- and alkylacetylenes. Pd-2(dba)(3)/P(t-Bu)(3) and CuI provide the best catalyst for reactions in re-fluxing THF and in the presence of K2CO3.
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