期刊
SYNTHESIS-STUTTGART
卷 -, 期 17, 页码 2845-2848出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2004-834871
关键词
1-arylethanones; 1-aryl-2,2-dichloroethanones; chlorination; hydrogen peroxide
1-Arylethanones are readily chlorinated with an aqueous HCl-H2O2 system using ethanol as a cosolvent. The reaction proceeds rapidly and results in selective conversion of 1-arylethanones into 1-aryl-2,2-dichloroethanones in yields of 48-89%, depending on the nature of the substituent in the aryl group.
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