期刊
CHEMISTRY-A EUROPEAN JOURNAL
卷 11, 期 2, 页码 719-727出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.200400754
关键词
aldehydes; amidation; radical reactions; surfactants; thioesters
The combination of the water-soluble radical initiator, 2,2'-azobis[2-(2-imidazolin-2-yl)propane] dihydrochloride (VA-044) and the surfactant, cetyltrimethyl-ammonium bromide (CTAB), was found to be the most suitable condition for the effective and direct synthesis of useful active thioesters (pentafluorophenyl thioesters) in water. In addition, the direct amidation of aldehydes was achieved by the addition of the amines to the thioesterification reaction mixture in water.
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