期刊
TETRAHEDRON
卷 61, 期 11, 页码 2871-2877出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2005.01.086
关键词
radicals; cyclizations; pyrrolidinones; rearrangements
The rearrangement of a trichloro-pyrrolidin-2-one, prepared by the CuCl-TMEDA catalyzed atom transfer radical cyclization of N-alkyl-N-(3-chloro-2-propenyl)-2,2-dichloromyristamide, with n-propylamine or CH3ONa/CH3OH, is the key step of a new, short and inexpensive route to chaetomellic anhydride C and (+/-)-erythro-roccellic acid. (c) 2005 Elsevier Ltd. All rights reserved.
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