期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 70, 期 10, 页码 4180-4183出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo050207g
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Chiral diols are important molecules with widespread use as chiral auxiliaries and ligands in enantioselective synthesis. Therefore, efficient and practical syntheses of highly dissymmetrical nonracemic diols are still a meaningful pursuit. Two new routes to access camphor-derived chiral diol 1 have been developed. One route employs camphorquinone (3) as the starting material, affording in only two steps the desired diol in 55% overall yield. The second route, from camphor (2), leads to the desired diol in an efficient four-step synthesis, with an overall yield of 55%.
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