期刊
CARBON
卷 43, 期 7, 页码 1386-1391出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.carbon.2005.01.005
关键词
fullerene; graphite; doping; transmission electron microscopy; X-ray diffraction
Carbon nitrides with graphite-like or onion-like lamellar structures were synthesized at low temperatures by the reactions of cyanuric chloride (C3N3Cl3) with NaNH2, K, or NaN3. The synthesized samples were investigated by powder X-ray diffraction, elemental analysis (from C-N combustion), X-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, Raman spectroscopy, mass spectroscopy, field-emission scanning electron microscopy, transmission electron microscopy, and high-resolution electron microscopy. The synthesized carbon nitride with a graphite-like lamellar structure was obtained and observed for the first time. The formation mechanism of the carbon nitride was discussed. (c) 2005 Elsevier Ltd. All rights reserved.
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