期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2005, 期 15, 页码 3177-3181出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.200500279
关键词
biaryls; cross-coupling; solid-phase synthesis; sulfonate; traceless multifunctional cleavage
Nickel-catalyzed reactions between polymer-bound arene-sulfonates and aryl Grignard reagents produce unfunctionalized biphenyls and terphenyls in good yields through reductive cleavage/cross-coupling of the C-S bond. This novel traceless multifunctional cleavage strategy appears to be a powerful tool for the preparation of large oligophenyl libraries, because it allows the introduction of diversity concomitantly with the release of the target compounds. ((c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2005).
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