期刊
ORGANIC LETTERS
卷 7, 期 17, 页码 3621-3624出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol050975u
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资金
- NCI NIH HHS [R01 CA059703, CA 59703, R29 CA059703] Funding Source: Medline
[GRAPHICS] Tungsten-catalyzed cycloisomerization of alkynyl alcohols including 8 provides only the endocyclic enol ether (11) as a key intermediate for the branched C-glycoside substructure (2) of altromycin B. A sequence of Stille cross-coupling reaction and regio- and stereoselective functional group transformations affords each C13-diastereomer of the branched C-arylglycoside (2a and 2b).
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