期刊
MATERIALS RESEARCH BULLETIN
卷 40, 期 9, 页码 1617-1622出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.materresbull.2005.04.033
关键词
nanostructures; sol-gel chemistry; X-ray diffraction
Barium hydroxyapatite (BaHAP) nanoparticles have been synthesized by citric acid sol-gel combustion method using citric acid as a reductant/fuel and nitrate as an oxidant at a relatively low temperature of 600 degrees C. The thermal decomposition of nitrate-citrate xerogel was investigated by thermogravimetric/differential thermal analysis (TG/DTA) technique. The yielding powders calcined at 600 degrees C have been characterized by Fourier transform infrared (FT-IR), X-ray diffraction (XRD), and transmission electron microscope (TEM). The possible combustion process was presented. (C) 2005 Elsevier Ltd. All rights reserved.
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