期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2005, 期 23, 页码 5024-5030出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.200500473
关键词
tunicates; ascidians; natural products; quinones; NMR spectroscopy; density functional calculations; GIAO
A chemical investigation of a Mediterranean ascidian, Aplidium conicum, has resulted in the isolation of the new metabolites aplidinone A (1), B (2), and C (3). The structures of aplidinones A-C were determined by interpretation of spectroscopic data, whereas the regiochemistry was determined by the comparison of experimental C-13 NMR chemical shifts with those predicted by GIAO shielding calculations. (c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2005.
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