期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 70, 期 25, 页码 10588-10591出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo0518598
关键词
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Nucleoside monophosphates, when activated by trifluoroacetic anhydride and N-methylimidazole, efficiently couple with a variety of electron-deficient diphosphonates in a reproducible and efficient manner (< 2 h, > 72% isolated yield). Unlike traditional methods for the preparation of nucleoside 5'-beta,gamma-methylenetriphosphate analogues, there is no requirement for predrying, or conversion to specific salt forms, of commercially available nucleoside monophosphate starting materials.
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