期刊
TETRAHEDRON LETTERS
卷 46, 期 51, 页码 8959-8963出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2005.10.041
关键词
bromination; hexamethylenetetramine-bromine; silica gel supported
A regioselective and highly efficient method for bromination of aromatic compounds in the presence of a stoichiometric amount of hexamethylenetetramine-bromine (HMTAB) as an efficient reagent in dichloromethane is reported. The selectivity depends on the temperature and nature of the substituent on the substrate. The reactivity of this reagent was increased by supporting it to silica gel for bromination of less activated compounds. (c) 2005 Elsevier Ltd. All rights reserved.
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