期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 71, 期 1, 页码 135-141出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo051878h
关键词
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The synthesis of nitrogen-containing heterocycles from alkyl dihalides (ditosylates) and primary amines and hydrazines via a simple and efficient cyclocondensation in an alkaline aqueous medium that occurs under microwave irradiation is described. This improved greener synthetic methodology provides a simple C C and straightforward one-pot approach to the synthesis of a variety of heterocycles, such as substituted azetidines, pyrrolidines, piperidines, azepanes, N-substituted 2,3-diliydro-1H-isoindoles. 4,5-dihydropyrazoles, pyrazolidines, and 1,2-dihydrophthalazines.
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