4.6 Article

Controlled synthesis of highly ordered LaFeO3 nanowires using a citrate-based sol-gel route

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MATERIALS RESEARCH BULLETIN
卷 41, 期 2, 页码 274-281

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PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.materresbull.2005.08.022

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inorganic compounds; nanostructures; chemical synthesis; sol-gel chemistry

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Highly ordered LaFeO3 nanowires of complex oxide were controlled synthesized with a porous anodic aluminum oxide (AAO) template by a citrate-based sol-gel route. The results of scanning electron microscopy (SEM) and transmission electron microscopy (TEM) revealed that the LaFeO3 nanowires formed a uniform length and diameter, which were determined by the thickness and the pore diameter of the AAO template, respectively. The results of X-ray diffraction (XRD) and the selected area electron diffraction (SAED) indicated that the LaFeO3 nanowires had a perovskite-type crystal structure. Furthermore, X-ray photoelectron spectroscopy (XPS) demonstrated that stoichiometric LaFeO3 was formed. (c) 2005 Elsevier Ltd. All rights reserved.

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