期刊
TETRAHEDRON LETTERS
卷 47, 期 14, 页码 2315-2317出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2006.02.021
关键词
thionation; thioamide; phosphorus pentasulfide; alumina
Alumina encapsulated phosphorus pentasulfide (P4S10/Al2O3) was found to be an efficient solid supported reagent for the thionation of long chain amides. This method is advantageous in terms of use of inexpensive reagent, simple reaction processing, and clean product in good to excellent yield. (c) 2006 Elsevier Ltd. All rights reserved.
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