期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 348, 期 7-8, 页码 846-850出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.200606022
关键词
alkynylation; amination; 1,2-dihalobenzenes; indoles; palladium; phosphane ligands
A simple, efficient palladium(II) acetate/tri-tert-butylphosphine-catalyzed indole synthesis from o-alkynylhalobenzenes, readily available from 1,2-dihalobenzenes, has been achieved in good to excellent yields. A one-pot, Pd(OAc)(2)/t-Bu3P-catalyzed sequential reaction from 1-chloro-2-iodobenzene, phenylacetylene and amines has also been achieved in good yields.
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