A novel 3D metal-organic framework [Cd-2(m-bptc)(4,4'-bpy)(0.5)(H2O)(4)]center dot H2O (1; m-H(4)bptc = 1,1'-biphenyl-2,3',3,4'-tetracarboxylic acid, 4,4'-bpy = 4,4'- bipyridine) with interweaving of triple- and single-helical chains has been obtained based on hydro(solvo)thermal reactions.
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