期刊
ELECTROANALYSIS
卷 18, 期 11, 页码 1126-1130出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/elan.200503488
关键词
voltammetry; solid electrodes; ink film; disposable sensor
The covering of conventional solid electrode with a film using an ink containing a conductive powder and a polymer enables to broaden the potential window of the original solid electrode. A solid silver amalgam electrode covered with such a film exhibits a potential window from -600 mV to +1400 mV vs. SCE reference electrode. The renewal of the film is fast and simple: the electrode can be simply wiped with a filter paper to remove the old film and immersed into an ink solution or 1-2 mu L of this ink solution can be applied to the surface of the electrode with a micro dispenser to form a new film. Therefore, just the inexpensive film at the electrode surface is disposable and there is no need to dispose the whole, more expensive electrode. Moreover, when a suitable electrochemical pretreatment of the film electrode is applied, the same film can be used for reproducible measurements for several days.
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