Two new mixed-metal metallaborane clusters, Cp*(Ru2IrB5H9)-Ru-3 and Cp*3Ru2IrB5H5, were isolated from the reaction of an iridaborane with a ruthenaborane. The structures show the former to have an unusual nido eight-atom cluster shape with a low electron count and the latter to have the expected bicapped-octahedral geometry.
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