期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 71, 期 12, 页码 4544-4548出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo0605290
关键词
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The Cadiot-Chodkiewicz coupling of cis-1,4-diethynyl-1,4-dimethoxycyclohexa-2,5-diene and the corresponding ethynyl bromide gave a mixture of acetyenic macrocycles ranging from dimer to octamer in good isolable yields. The trimeric and tetrameric macrocycles have been structurally characterized by single-crystal X-ray crystallography. In the crystal structure of the trimeric macrocycle a molecule of benzene is sandwiched between a pair of macrocyles. The tetrameric macrocycle exhibited a tub-shaped conformation and encapsulated a molecule of ethyl acetate inside the tub.
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