期刊
ORGANIC LETTERS
卷 8, 期 13, 页码 2667-2670出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol0604015
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资金
- NIGMS NIH HHS [GM-18874] Funding Source: Medline
The resolution in the lithiation-substitution sequence from 1 to 4-11 in MTBE is shown to be under thermodynamic control in contrast to the previous report of kinetic control in diethyl ether. Diastereomeric equilibration of a soluble complex is shown to be controlling and an asymmetric synthesis of a 3,4,5-substituted benzazepine is reported.
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