期刊
MOLECULES
卷 11, 期 7, 页码 523-527出版社
MOLECULAR DIVERSITY PRESERVATION INTERNATIONAL
DOI: 10.3390/11070523
关键词
hypervalent iodine; alpha-azido ketones; [hydroxy(tosyloxy)iodo]benzene; iodosobenzene
Reaction of various ketones with [hydroxy(tosyloxy)iodo]benzene (HTIB) followed by treatment of the alpha-tosyloxy ketones thus generated in situ with NaN3 offers a one-pot procedure for the synthesis of alpha-azido ketones. The HTIB used in this conversion may also be generated in situ by using iodosobenzene in combination with p-toluene-sulphonic acid.
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