期刊
JOURNAL OF CHEMICAL TECHNOLOGY AND BIOTECHNOLOGY
卷 81, 期 7, 页码 1271-1276出版社
JOHN WILEY & SONS LTD
DOI: 10.1002/jctb.1545
关键词
cyclodextrin; removal of phenols; diisocyanate network polymer; industrial wastewater
Removal of phenolic compounds from a raw industrial wastewater from phenolic resin processing, of which the components are phenol (8.9 wt%), m- and p-cresols (0.33 wt%), and xylenols (0.044 wt%), was carried out by using crosslinked cyclodextrin particles as a sorbent. A series of sorbents was prepared by varying the combination of cyclodextrin (CyD), beta-CyD, gamma-CyD, Mix-CyD (alpha-CyD:beta-CyD:gamma-CyD:dextrin = 30:10:10:SO wt/wt), the crosslinker, hexamethylene diisocyanate (HDI) or toluene-2,6-diisocyanate, and their molar ratio in the reaction batch. The removal of the phenolic compounds from raw industrial wastewater was an instantaneous process and was completed within about 5 min. The best removal efficiency was obtained by the crosslinked beta-CyD with HDI in a 1:8 molar ratio or the crosslinked Mix-CyD with HDI, also in a 1:8 molar ratio. The prepared sorbents were efficiently regenerated by elution of the adsorbed phenols from the crosslinked polymers with methanol. (c) 2006 Society of Chemical Industry.
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