期刊
ORGANIC LETTERS
卷 8, 期 15, 页码 3315-3318出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol0611752
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资金
- NIGMS NIH HHS [GM-29028] Funding Source: Medline
The total synthesis of the marine diolide (-)-clavosolide A has been achieved in 17 steps (longest linear sequence) from commercially available crotonaldehyde exploiting the Petasis-Ferrier union/rearrangement tactic to construct the requisite aglycon monomer. A one-pot esterification/lactonization employing the Yamaguchi protocol, followed by bis-glycosidation, furnished (-)-clavosolide A.
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