期刊
ORGANIC LETTERS
卷 8, 期 15, 页码 3251-3254出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol061057e
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资金
- NIGMS NIH HHS [R01 GM67173] Funding Source: Medline
Palladium(II) catalyzes the oxidative coupling of allyl tosylamides with butyl vinyl ether and various styrene derivatives to produce 2,4-substituted pyrrolidine products at room temperature. Molecular oxygen together with a copper(II) cocatalyst mediates reoxidation of the palladium catalyst. The reactions with styrene substrates can be performed in an open flask with ambient air as the source of O-2. Several nontraditional cocatalysts, including catechol, cyclooctadiene, and methyl acrylate, have a beneficial effect on the reactions.
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