期刊
TETRAHEDRON
卷 62, 期 31, 页码 7455-7458出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2006.05.017
关键词
D-gulono-1,4-lactone; L-gulono-1,4-lactone; 5,6-O-sulfinyl-1,4-lactone; 6-amino-6-deoxy-D-gulonolactam; 6-amino-6-deoxy-L-gulonolactam
Syntheses of 6-amino-6-deoxy-2,3-0-isopropylidene-D-gulono- and L-gulono-1,6-lactams 3 and 4 from corresponding glycono-1,4-lactones are described. Activation of the primary hydroxyl group requires 5,6-cyclic sulfite intermediate to obtain 6-azido-6-deoxy derivatives, which are cyclized after reduction. (c) 2006 Elsevier Ltd. All rights reserved.
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