期刊
TETRAHEDRON-ASYMMETRY
卷 17, 期 14, 页码 2064-2068出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetasy.2006.07.023
关键词
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Various L-prolinamides 14, prepared from L-proline and chiral beta-amino alcohols, are active bifunctional catalysts for the direct nitro-Michael addition of ketones to beta-nitrostyrenes. In particular, catalyst 14e prepared from L-proline and (1S,2R)-cis-1amino-2-indanol exhibits the highest catalytic performance working in polar aprotic solvents such as NMP. High syn-diastereoselectivities (up to 94% de) and good enantioselectivities (up to 80% ee) were obtained at rt. (c) 2006 Elsevier Ltd. All rights reserved.
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