期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 71, 期 18, 页码 7110-7112出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo061160h
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资金
- NIGMS NIH HHS [GM 54051] Funding Source: Medline
Addition of lithium acetylides prepared from 1-pentyne, phenylacetylene, and trimethylsilylacetylene to diverse N-tert-butanesulfinyl ketimines affords a range of alpha, alpha-dibranched propargyl sulfinamides in generally good yields (up to 87%) and with high diastereoselectivities (up to > 99: 1). Acidic cleavage of the tert-butanesulfinyl group provides the free alpha, alpha-dibranched propargylamines.
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