期刊
QUIMICA NOVA
卷 29, 期 5, 页码 926-931出版社
SOC BRASILEIRA QUIMICA
DOI: 10.1590/S0100-40422006000500008
关键词
micelar electrokinetic chromatography; amphenicols; milk
A micellar electrokinetic chromatographic method (MEKC) is described for determining residues of amphenicols(chloramphenicol,thiamphenicol and florfenicol) in bovine milk. MEKC is conducted by using a separation buffer consisting of 20 mM Na2HPO4, 10 mM Na2B4O7, 50 mM SDS at pH 8.0; UV detection at 210 nm and 10 kV of voltage. The limit of detection ranged from 4.3-5.3 mu g L-1. The MEKC method was applied for the simultaneous determination of amphenicols in milk samples spiked with amphenicols at three concentration levels: 10, 30 and 50 mu g L-1. Recoveries ranging from 91-105% were obtained by following a simple extraction/preconcentration procedure.
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