期刊
ORGANIC LETTERS
卷 8, 期 21, 页码 4879-4882出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol061938l
关键词
-
资金
- NIGMS NIH HHS [R01 GM062160, R01 GM062160-07, GM 57335, R01 GM057335] Funding Source: Medline
[GRAPHICS] The (1-naphthyl) propargyl group is introduced as a sterically unobtrusive alcohol protecting group that is cleaved in a single step by exposure to dichlorodicyanoquinone in wet dichloromethane. In conjunction with the 4,6-O-benzylidene protecting group, and the use of the sulfoxide glycosylation method, 3-O-naphthylpropargyl-protected mannosyl donors are extremely beta-selective.
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