期刊
BIOORGANIC & MEDICINAL CHEMISTRY LETTERS
卷 16, 期 20, 页码 5324-5327出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.bmcl.2006.07.083
关键词
aldehydes; magnesia; solvent-free; phosphorylation; acetic anhydride
A simple, efficient, and new method has been developed for the synthesis of alpha-acetoxyphosphonates from aldehydes through a one-pot reaction of aldehydes with diethylphosphite in the presence of acetic anhydride under solvent-free conditions using magnesium oxide. This method is easy, rapid, and high yielding for the one-pot synthesis of alpha-acetoxyphosphonates from aldehydes. (c) 2006 Elsevier Ltd. All rights reserved.
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