期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2006, 期 21, 页码 4898-4904出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.200600564
关键词
rhodium; homogeneous catalysis; hydroboration; boranes; olefins
Rhodium-catalyzed hydroboration of 1-octene and trans-4-octene with sulfur- and nitrogen analogues of catecholborane are demonstrated with the use of in situ B-11 NMR spectroscopy. Our study shows that the sulfur- and nitrogen analogues are significantly less prone to disproportionation than catechol, which results in enhanced yields of the desired compounds. ((c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2006).
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