期刊
SYNLETT
卷 -, 期 18, 页码 2953-2958出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2006-951512
关键词
palladium; Heck reaction; catalysis; solvent-free; microwave
The rapid, microwave-promoted Heck coupling of aryl iodides in open reaction vessels is presented and scale-up of the reactions to the mol scale demonstrated. Reactions are performed using 0.1 mol% palladium acetate as the catalyst, sodium carbonate and tributylamine as bases and tetrabutylanimonium bromide as an additive.
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