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Hydrothermal synthesis of molybdenum oxide based materials: Strategy and structural chemistry

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CHEMISTRY-A EUROPEAN JOURNAL
卷 12, 期 36, 页码 9122-9134

出版社

WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.200600977

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hydrothermal synthesis; in situ spectroscopy; molybdenum oxide; nanostructures; polyoxometalates

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The preparative flexibility of hydrothermal syntheses needs to be systemised for exploring complex structure-synthesis relationships and morphology control options in materials chemistry. This is demonstrated for the targeted hydrothermal preparation of molybdenum oxide materials: firstly, in situ studies were employed for the efficient production of MoO3 nanofibfes. Furthermore, ionic substances as structure-directing tools brought forward a new class of fluorinated polyoxomolybdates.

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