期刊
TETRAHEDRON LETTERS
卷 47, 期 52, 页码 9211-9213出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2006.10.134
关键词
N-phenyltriazolinedione; oxidation; thiols; disulfides
N-Phenyltriazolinedione is an efficient and chemoselective reagent for the oxidation of thiols to their corresponding symmetrical disulfides. The method is applicable to aromatic, aliphatic, and bi-functional thiols. The one-pot reaction takes a few minutes (in most cases studied) for completion and after a simple work-up affords the corresponding symmetrical disulfides in very good to excellent yields. Furthermore, the reaction could be performed with the same results in the absence of solvent for liquid thiols. (c) 2006 Elsevier Ltd. All rights reserved.
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