期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 129, 期 3, 页码 508-509出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja068271i
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The new macrolide spirastrellolide B (5) has been isolated from extracts of the marine sponge Spirastrella coccinea collected in Dominica. Chemical transformations of spirastrellolide B have converted it to a bromine-containing crystalline derivative 8 that has a truncated side chain. Singlecrystal X-ray diffraction analysis of the derivative 8 has revealed the absolute configuration of the macrolide core of spirstrellolide B to be 3R,7S,9S,11S,13R,14S,17S,20S,21R,22S,23S,24S,27R,29S,31R,34S,35R,37S,38S.
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