期刊
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
卷 53, 期 35, 页码 9321-9324出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201404120
关键词
C-N coupling; copper; heterogeneous catalysis; mechanosynthesis; synthetic methods
资金
- NSERC
- FRQNT Nouveaux Chercheurs fund
- Canada Foundation for Innovation Leader's Opportunity Fund (CFI-LOF)
- Tak-Hang (Bill) and Christina Chang Fellowship
- NSERC CREATE
Reported herein is the mechanochemical synthesis of sulfonyl guanidines, a family of molecules which are relevant as pharmaceuticals and herbicides, by direct coupling of sulfonamides and aromatic or aliphatic carbodiimides. Attempts to conduct the coupling in solution have either failed or given very low conversions, thus demonstrating mechanochemistry as the necessary component for the discovery of this synthetic strategy.
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