期刊
PHYSICA B-CONDENSED MATTER
卷 390, 期 1-2, 页码 59-64出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.physb.2006.07.062
关键词
ceria; nanowires; alcohothermal synthesis
Well monodispersed and large-scaled ceria nanowires with cubic fluorite structure and high aspect ratios were successfully prepared at 80 degrees C without further sintering via a facile surfactant-assisted alcohothermal route. The X-ray diffraction, transmission electron microscopy with selected-area electron diffraction indicated that the as-prepared ceria nanowires had a cubic fluorite-structure and the morphologies of the products were uniform, with diameters of about 50-100 nm. The TG-DTA and XPS measurements revealed the existence of both trivalent and quadrivalent cerium and an oxidization process took place gradually with increase of the reaction time. Compared with as-reported method, the present process is more convenient and feasible. (c) 2006 Elsevier B.V. All rights reserved.
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